Just crush the crucible really fine and cover with nitric.Have been cooking over and over more than 40 x times, there are plenty of Flux been used.
Yes, you are right. Have been missing 2 oz of Ag and the crucible is eating them ... lol
A price to pay I guess.![]()
Filter solution, add HCl, AgCl precipitates out, filter again and you can either convert to AgO (safer, doesn't give off chlorine) or thermally decompose as is to release the gas and liberate your silver.
If you have used gold or platinum in the crucibles after you've initially used nitric to get the silver out, you'll need to cover what's left with Aqua Regia and recover that way.
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